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Or at work. Or anywhere else for that matter. There are a lot of oxidization reactions available, but in this case we of course want something that will produce the Markovnikov product , with addition occurring at the more substituted end of the alkene. An initial oxidation to an alcohol followed by a second oxidation step to a ketone is also a possibility. Since safrole and PMK are carefully watched and regulated precursors, the current favorite precursor typically bought from Chinese chemical manufacturers is PMK glycidate. PMK glycidate can reportededly be easily broken down into PMK simply by refluxing it with hydrochloric acid. But read on about the chemical watch lists! Step 2 : Reversible imine formation occurs spontaneously when the ketone is placed in solution with methylamine freebase not the hydrochloride salt. Step 3 : Reduction via hydrides, aluminum-mercury amalgams, or electrical cells or catalytic hydrogenation permanently converts the imine to MDMA. All MDMA sold on the streets appears to be racemic. A product containing only one isomer would not subjectively feel the way racemic MDMA does, being either more amphetamine-like or more sedating and mellow like MDEA , which seems to be primarily a serotonin releaser. Even attempting to order one of these chemicals can bring law enforcement attention. Isomerization of safrole is reportedly an easy operation, as described in the famous Strike synthesis collection. A more compact review can be found in this old doc saved from Rhodium. Mercury-aluminum amalgam is an interesting little reagent. Aluminum has a low electronegativity, which suggests that it would react very readily with anything mildly electron-hungry such as the carbon atom of an imine, or the hydrogen atoms of water. This aluminum oxide forms a tightly interlocking crystalline layer over the remaining aluminum, sealing it off and protecting it from further reactions. Mercury is able to penetrate this protective oxide layer and prevent it from re-forming, which allows the aluminum to continue to react, contributing electrons to reduce whatever suitable chemical oxygen, water, imines, etc. He vacuum distills it or perhaps uses fractional freezing to isolate the safrole, yielding about 40 ml of safrole. Purified safrole is suspicious in any quantity and should never be ordered. This would normally be done with oxygen gas, but a less hardware-intensive method is to use benzoquinone as the oxidizer. So, in a ml round bottom flask the daring cook mixes together:. As an exercise for students, try synthesizing PdCl2 from palladium metal with aqua regia. After throwing in a magnetic stir bar, they stirred this mixture for at least an hour preferably longer to dissolve the benzoquinone. At this point, the flask would be fitted with a reflux condenser and the 40 ml safrole slowly added over the course of an hour. The addition funnel might be rinsed down with methanol to ensure he got all the safrole out. Once all the safrole was added, the solution was kept heated to a gentle reflux with stirring for at least 8 hours. After cooling, the solids were filtered off and are a waste product. The ketone produced by the reaction was extracted with DCM or another organic solvent and purified through vacuum distillation, giving perhaps 25 ml of a light yellow colored oil. After mixing the ketone with some methylamine freebase, a responsible and well equipped chemist would likely just use a hydride to reduce it to MDMA. First, they would need to prepare a solution of methylamine freebase. This reaction is very exothermic and must be done slowly with an ice water bath to cool the solution. The colder the solution is, the less offgassing. Methylamine is, to use the legal terminalogy, suspicious as holy fuck. In a 1, ml round bottom flask, place 12 g of pieces of heavy duty aluminum foil the stuff used in the kitchen. Toss in a large stir bar. Dissolve mg of HgCl2 mercury chloride in ml methanol. Add this solution to the flask containing the aluminum. This will start the reaction that forms the mercury-aluminum amalgam. The foil will turn gray, then start to release bubbles of hydrogen gas. HgCl2 mercury chloride is regulated and watched being both suspicious and very, very poisonous. Tiny amounts can be obtained by breaking open mercury tilt switches. Mercury metal, like palladium, can be oxidized to a chloride salt with aqua regia. Once the amalgam started to bubble see video , they would add the methylamine solution and their 25 ml of PMK. This is reported to be a moderately exothermic reaction; it may want to boil without adding any heat, but should be easily contained by the reflux condenser. Once the reaction calms down, heat can be added to gently reflux the solution for another 4 hours. Once the reaction is done, the reaction flask is flooded with g of sodium hydroxide dissolved in ml distilled water and the whole mess extracted with a non-polar solvent such as a few hundred ml of toluene. The extraction solvent is washed with distilled water, then saturated salt solution, and finally dried with some perhaps g dehydrated magnesium sulfate epsom salts. If everything has worked out, the lucky chemist now has perhaps g of MDMA freebase an oil dissolved in toluene or some other solvent. The classic next step would be to bubble hydrogen chloride gas through the solvent to form MDMA hydrochloride the crystals you see sold on the market. The solvent is distilled off, leaving the crude MDMA freebase in the flask. It could be further purified by vacuum distillation, but that seems unnecessary. This crude product is dissolved in 80 ml of dry isopropanol isopropyl alcohol. Concentrated hydrochloric acid is added a drop at a time until the solution turns slightly acidic. At this point, MDMA hydrochloride has formed. To get it to crash out of solution, ml of dry ether is added. After letting the solution sit and perhaps cool in the freezer , the crystals that formed could be filtered off and dried. And that would be it; MDMA crystals. Molly ahoy! The pot of gold at the end of a long, difficult, legally and otherwise perilous road. Assuming the cook has gotten all of the reactions to work correctly, of course. If you want drugs, buy them. If you want a good income source, stay in college and get a decent professional job. There are three sections to the list of regulated precursors. Instead, the law applies to importers, manufacturers, and distributers. The import restriction can trip people up. Unless the seller has deliberately mis-labeled the oil as something unregulated, US Customs will notice your little purchase as it enters the US and pass on the information to the Drug Enforcement Administration. Any time you mail-order a List 1 chemical the seller is supposed to report your purchase to the DEA. Supposed to. Whether that happens reliably on, say, eBay is another question, but hobbyist chemists should give it some serious thought before ordering a List 1 chemical. If your company makes or sells an item on this list, you are expected to report on your inventory, etc. Do the guys selling pill presses on eBay or the many other markets actually do this? Maybe, maybe not. Although many chemicals are closely watched, glassware and most lab equipment is generally unwatched and unrestricted, although there are some local exceptions. Texas has particularly crazy laws on glassware. Apparently nobody told them that most of their meth comes from Mexican super-labs. The takeaway point should be that getting the materials needed to run a drug lab can be a complicated, expensive process and a legal landmine. Even very smart, very well financed criminal organizations get caught now and then. For the average person say, an enthusiastic young chem major it can verge on a death wish. Chemical reactions can produce large amounts of strong, suspicious smells and vapors, making a lab very difficult to hide. Reactions can be violent, running out of control like a wildfire. And law enforcement is always on the lookout for suspicious purchases of equipment and chemicals. I would strongly advise any reader to not go down this particular path. If something a little more brilliantly ghetto is your thing, Chem Player has some great stuff. For something more interactive, you might like the forums over at Science Madness where openly discussing making illegal drugs is not allowed, but all sorts of other things are. Well, to brass tacks. So, in a ml round bottom flask the daring cook mixes together: 40 g p-benzoquinone ml methanol 0.

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MDMA is an even more stable molecule; it doesn’t absorb any moisture from the air at all. According to Jones, 'Unless it is literally damp to the touch, it will probably outlive a human, no matter what. If you leave it in direct sunlight it might slowly break down, but if you just store it in any normal place then it's not going to break down in any way.

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