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Subject: 1 selected item: 30444599 - PubMed
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Affiliations
1 State Key Laboratory of Precision Measurement Technology and Instruments, Department of Precision Instrument , Tsinghua University , Beijing 100084 , China.
2 PURSPEC Technologies Inc. , Beijing 100084 , China.
Affiliations
1 State Key Laboratory of Precision Measurement Technology and Instruments, Department of Precision Instrument , Tsinghua University , Beijing 100084 , China.
2 PURSPEC Technologies Inc. , Beijing 100084 , China.
Miniature mass spectrometers are of an increasing interest for in-situ analyses, and their coupling with the ambient ionization sources is a valid path for direct analysis of complex samples. In this study, a miniature mass spectrometer using discontinuous atmospheric pressure interface was developed with a dual-LIT (linear ion trap) configuration. The comprehensive scan modes were enabled for tandem mass spectrometry analysis, which are critical for high-quality qualitative and quantitative analysis. A real-time pressure control was implemented to facilitate the ion transfer and collision induced dissociation (CID). Beam-type CID could be performed for tandem analysis at a high number of stages. In-trap CID at high q could also be performed with the fragment ions accumulated in a second trap. A precursor ion scan mode for analyzing target analytes has also been demonstrated.
Chen TC, Xu W, Ouyang Z. Chen TC, et al. Rapid Commun Mass Spectrom. 2011 Nov 15;25(21):3274-80. doi: 10.1002/rcm.5226. Rapid Commun Mass Spectrom. 2011. PMID: 22006390
Gao L, Li G, Cooks RG. Gao L, et al. J Am Soc Mass Spectrom. 2010 Feb;21(2):209-14. doi: 10.1016/j.jasms.2009.10.005. Epub 2009 Oct 12. J Am Soc Mass Spectrom. 2010. PMID: 19892569
Kang M, Zhang W, Dong L, Ren X, Zhu Y, Wang Z, Liang L, Xue J, Zhang Y, Zhang W, Ouyang Z. Kang M, et al. Anal Chim Acta. 2020 Mar 8;1101:74-80. doi: 10.1016/j.aca.2019.12.028. Epub 2019 Dec 13. Anal Chim Acta. 2020. PMID: 32029121
Patel DN, Li L, Kee CL, Ge X, Low MY, Koh HL. Patel DN, et al. J Pharm Biomed Anal. 2014 Jan;87:176-90. doi: 10.1016/j.jpba.2013.04.037. Epub 2013 May 6. J Pharm Biomed Anal. 2014. PMID: 23721687 Review.
Laskin J, Futrell JH. Laskin J, et al. Mass Spectrom Rev. 2003 May-Jun;22(3):158-81. doi: 10.1002/mas.10041. Mass Spectrom Rev. 2003. PMID: 12838543 Review.
Wang Y, Zhang W, Ouyang Z. Wang Y, et al. Chem Sci. 2020 Sep 10;11(38):10506-10516. doi: 10.1039/d0sc03237a. Chem Sci. 2020. PMID: 34094309 Free PMC article.
Foreman DJ, Bhanot JS, Lee KW, McLuckey SA. Foreman DJ, et al. Anal Chem. 2020 Apr 7;92(7):5419-5425. doi: 10.1021/acs.analchem.0c00146. Epub 2020 Mar 9. Anal Chem. 2020. PMID: 32100997 Free PMC article.
Li M, Liu X, Zhou X, Ouyang Z. Li M, et al. J Am Soc Mass Spectrom. 2019 Dec;30(12):2750-2755. doi: 10.1007/s13361-019-02344-x. Epub 2019 Oct 28. J Am Soc Mass Spectrom. 2019. PMID: 31659717
Zou R, Cao W, Chong L, Hua W, Xu H, Mao Y, Page J, Shi R, Xia Y, Hu TY, Zhang W, Ouyang Z. Zou R, et al. Anal Chem. 2019 Jan 2;91(1):1157-1163. doi: 10.1021/acs.analchem.8b04935. Epub 2018 Dec 19. Anal Chem. 2019. PMID: 30525456 Free PMC article.
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