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Amphetamine Synthesis Amphetamine Synthesis. Ammonia Synthesis Full description. Methadone Synthesis A Presentation and detailed instruction for medicinal chemistry on the synthesis of Methadon, an opiate used worldwide to treat addiction. Synthesis Paper hghjhFull description. This is for theoretical argument only. In no way do I condone this activity. This is a hypothetical synthesis for: The synthesis as described 1. The synthesis itself can be performed in a series of weekends or in a straight shot. Be prepared to read and learn. Read the whole thing before you start. This list is the basics. A must, throughout this text, pages from this book will be mentioned. These are the best. But aspirators are cheap 1. Put one of your mL RB flasks as the receiving flask. Start turning up the heat slowly! You will get a good idea about how the pieces go together, and become familiar with the fragility of the whole thing. Read Zubrick for advise about where to place the clamp. A bowl with a flat bottom rests on the Hotplate. It is filled with Peanut Oil. The distillation flask sits in the bowl but not touching the bottom, so that the Hotplate heats the bowl, the bowl heats the Peanut Oil, the Peanut Oil heats the distillation flask. This is VERY effective. Set up for distillation not vacuum. In the distillation flask your mL RBFlask put: Remember to turn on the water in the condenser! Turn up the heat. Crystals should start to form in several minutes. Filter off these Ammonium Chloride Crystals. Distill off half of the remaining liquid. This is fine for the next step. It may be a little wet, but if you let it crystallize hot spontaneously in the flask with heat it should be fairly dry. Seal it in a wide mouth jar until needed. Another way is to put 20mL of water in a cup then add 5g of the NaOH to it. If you do the same with Ammonium Chloride, it will just smell like ammonia. This can be stored at room temperature, forever. HCl with excellent results. It uses PdCl2 as a catalyst to put and oxygen across a double bond. If you do this correctly, you will have more MDMA. HCl than you know what to do with. After the addition, the solution was dark reddish orange. This reaction requires NO additional heating! The oil fell out of solution to the bottom. This is when its nice to have a Big Sep Funnel. Now we need to define several things. The upper layer in this case! The upper aqueous layer was decanted from the oil IE it was poured off. You now should have about mL total of DCM washes. Pour the DCM washes and the Organic layer together. The NaOH layer Aqueous: Put several boiling stones in too. Set up for vacuum distillation. What temp did it come over for you? WEIGH the receiving flask! Write the weight on a piece of tape and tape it to the flask! This is the DCM coming off first. You are going to have to change the flask, when the temp gets to above the safrole temp. This is a bit tricky, because you are going to have to release the vacuum. IE with an aspirator, turn on the water slowly. With an aspirator you can vary the vacuum when you are turning it on. You simply turn on the water slowly. IE Increase water pressure slowly. Look at how it refracts light. It will become a very viscous liquid. Total waste of effort, time, and precursors. The ketone is unstable. And then it will be useless. After its in the freezer you can stop for today. This process utilizes the electronegative properties of the Aluminum. This is the oxidized form of Aluminum. We will remove this part of the foil so that the aluminum can reduce the imine with elemental Al. This reaction actually has two parts. Second, the imine is reduced Hydrogen is added across the double bond to the amine. What you need to have prepared ahead of time: This is so that you can put the heating plate and stirbar combo under it. Have your thermometer already in its thermometer adapter so you can throw it in the flask at any second. Prepare the following, put them in a jar and have them ready at a moments notice: Amalgamation was allowed to proceed until there was the evolution of fine bubbles the formation of a light grey precipitate, and the appearance of occasional silvery spots on the surface of the aluminum. This should take between 15 and 30 minutes. When amalgamation is complete, pour out the water into the milk jug. Pour it out into the jug. So basically, you wash the Al pieces with 2xmL of water. This will remove most of the Hg from the solution. So be quick and have the ingredients ready for the procedure. Now, immediately, add in THIS order: Put the thermometer in the solution. Start being very paranoid about the temperature. Stirring is necessary so, with the heat off, stirbar on, flask sitting in the cool water bath. The whole time you are doing this the contents are a grey sludge. Remember to keep the stirbar going! If the stirbar is difficult to start going. This reaction should go no less than 6 hours. Stir the contents some more, and then let the stirbar stop and then let the solution rest for at least 30 minutes. The NaOH solution will make that grey sludge into a filterable consistency. Then in a matter of minutes the whole thing will be resting on the bottom of your flask. The reaction contents will settle out. The grey sludge will settle to the bottom, and a clear yellow liquid will rise to the top. Pour off the clear yellow liquid. Pour off the 2nd clear yellow liquid once it settles. Add the 2nd clear yellow liquid to the first. Do this several times, or until the clear liquid is no longer yellow. This is an extraction out of the reaction contents. The more you do this process, the higher your yield. After you have gotten as much of the yellow liquid out as you could. Put the grey sludge in the same milk jug waste container. But you should dispose of it properly. Not down the sink. Set up for vacuum distillation Boiling Stones! Make sure you get the alcohol out. This works very well for our target molecule, and any molecule that contains an amino group. Stir or shake it up. A lot of the brown oil should go into the acid solution. Now pour into this solution 30mL of DCM. Shake again and let it settle. When you do this the Aqueous layer will turn a milky white and may heat up just a little bit. A light brown oil will fall out of the solution. This is your product in the freebase form. Shake and let it settle out. Wash the aqueous layer twice more with 50mL of DCM. Combine those DCM washes that contain your product, and continue. That should be good enough. Step 6 2 hours work 6. If its not, then you will not get crystals. If water is present, then you can expect to get crapola. This first step can be done ahead of time. Like, during a distillation or reaction: There might be a little heat evolution, but not to worry Shake it up and then let it sit till the MgSO4 settles out. Now shake the bottle and let it sit for 15 minutes. You can actually do this while you are distilling or waiting for a reaction to proceed. Pour it into the flask that contains the MDMA oil, and drop the stirbar in too. Stir the crystals to promote even heating. After the acetone wash, dry the crystals. You should have around 15g of dry crystals. And these crystals are ready for consumption. For me at least. If you have completed this, congrats. Now Teach Someone Else! Remember me Forgot password? SITE To ensure the functioning of the site, we use cookies. We share information about your activities on the site with our partners and Google partners: Your consent to our cookies if you continue to use this website.

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