Ai Serizawa
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Shibaura Institute of Technology · Department of Materials Science and Engineering
Materials Science and Technology Division Oak Ridge, United States
Department of Metallurgy and Ceramics Science Japan
Department of Metallurgy and Ceramics
Metal additive manufacturing is a powerful tool for providing the desired functional performance through a three-dimensional (3D) structural design. Among the material functions, anisotropic mechanical properties are indispensable for enabling the capabilities of structural materials for living tissues. For biomedical materials to replace bone func...
In this study, in order to evaluate the adhesion properties of the hydroxide film formed on 6061 alloy (Al-1Mg-0.6Si (wt.%)) sheets prepared by steam coating, we examined the microstructure and cracking behavior of hydroxide film on Al alloy sheets prepared by steam coating at 220℃ for 24 h. EBSD analyses revealed the steam-coated sample exhibits m...
Hydroxide film was formed on 6061 Al-alloy (Al-1.00Mg-0.62Si(wt.%)) sheets by steam coating with the temperature of 220 °C for 24 h. During bending test of the coated specimens, the crack initiation and propagation processes in the hydroxide film were investigated using in situ SEM observations. The hydroxide film formed exhibited a dual-layer stru...
To elucidate the adhesion properties of anticorrosion hydroxide films formed on aluminum (Al)-alloy sheets prepared by the steam coating process, cracks that propagated inside the hydroxide film formed on Al–Mg–Si alloy (6061 grade) sheets were characterized. Continuous hydroxide films with different thicknesses of 0.7 μm and 1.4 μm formed at diffe...
Mg alloys are expected to be used in fields of the transportation industry because of their lightweight property, however, they show low corrosion resistance. To improve the corrosion resistance, preparation of the protective film on Mg alloys is essential. In this study, composite hydroxide films were prepared on three types of Mg alloys with diff...
Microstructures and crystallographic features of layered double hydroxide (LDH) particles and the LDH film formed on the aluminum alloy sheet (alloy 7075) using the steam coating process were examined by transmission electron microscopy (TEM). The LDH powder particles exhibited a hexagonal-disc-shape morphology. Their disc plane and side planes wer...
Steam aging behavior of Al–Mg–Si alloys was investigated in order to clarify if steam could enable to induce precipitation. Age-hardening behavior was evaluated by Micro-Vickers hardness tests and differential scanning calorimetry (DSC). As a result of steam aging, that is an aging heat treatment utilizing thermal energy of steam, it was revealed t...
Corrosion resistant films with almost the same film thickness were prepared on the magnesium alloy AZ61 by steam coating at different vapor pressure and treatment times. The effect of the vapor pressure on the structures and the corrosion resistance of the films was investigated by using FE-SEM, SEM-EDX, GAXRD, and potentiodynamic polarization curv...
Corrosion-resistant films were fabricated on Al–Zn–Mg alloy by steam coating using an acidic aqueous solution of Zn(NO3)2 at different concentrations. X-ray diffraction patterns and Fourier transform-infrared spectrometer spectra demonstrated that nitrate-type Zn–Al layered double hydroxide (LDH) and ZnO films were formed on the Al–Zn–Mg surface by...
Corrosion resistant films were fabricated on Al-Zn-Mg alloy by steam coating using Zn(NO3)2 aqueous solution at different concentrations. XRD patterns and FT-IR spectra demonstrated that nitrate type Zn-Al layered double hydroxide (LDH) and ZnO films were formed on the Al-Zn-Mg alloys by steam coating at the temperatures of 373 to 433 and 473 K, re...
Al alloys offer excellent physical and mechanical properties, such as a low density, high specific strength, and good ductility. However, their low corrosion resistance has restricted their application in corrosive environments. There is a need, therefore, for a novel coating technology that is capable of improving the corrosion resistance of Al al...
Corrosion resistant films were prepared on flame-resistant Mg-6Al-1Zn-2Ca (in mass%) alloy by steam coating using ultra pure water as steam source. The prepared films were characterized using SEM, XRD, and FT-IR. Corrosion resistance of the film was estimated by polarization curve measurement in 5 mass% NaCl aqueous solution. All XRD patterns of th...
Corrosion resistant films were prepared on the Ca-added flame-resistant magnesium alloy AZCa612 by steam coating at different treatment time and temperature. The formation mechanism of the films was investigated by using the digital microscope, FE-SEM, XRD, FT-IR, XPS and the potentiodynamic polarization curve measurements in a 5 mass% NaCl aqueous...
In recent years, a reduction in weight of materials is highly desirable in the fields of transport industry and information technology devices. Magnesium (Mg) alloys have excellent physical and mechanical properties such as low density, good electromagnetic shielding, and high strength/weight ratio. Unfortunately, they have a great issue that is lo...
The effect of high densities of dislocations on the formation behavior of nanoscale clusters (nanoclusters), which are formed during natural aging at room temperature and the pre-aging at ~373 K in a 6000 series aluminum alloy, was investigated by atom probe tomography. Cold rolling was applied to modify the formation behavior and/or the characteri...
This chapter introduces a novel, chemical-free “steam coating” method for preparing films on magnesium (Mg) alloys and assesses their effectiveness in improving the corrosion resistance of two different Mg alloys. A film composed of crystalline Mg(OH)2 and Mg-Al layered double hydroxide (LDH) was successfully formed on AZ31 Mg alloy, and its corros...
Ti-15Zr-7.5Mo alloy was melted and its structure and mechanical properties were evaluated, followed by micro-arc oxidation (MAO) treatment to add bioactivity. Melted Ti-15Zr-7.5Mo alloy was consisted of mainly β containing of metastable α'' and ω phases. The Vickers hardness of the alloy was 420 HV and larger than those of Ti-6Al-4V alloy (320 HV)...
To develop high-temperature Ti alloys, microstructure and oxidation behavior were investigated in Ti-(10,15)Al-2Nb-(1,2)Zr (at%) alloys. For reference, ternary Ti-15Al-2Zr alloy was also investigated. A single α phase exists in Ti-10Al-2Nb-(1, 2)Zr alloys; on the other hand, an α and α2 two-phase was observed in Ti-15Al-2Nb-(1, 2)Zr alloys. Fine α2...
Halogen-doped carbon nanoparticles (CNPs) were synthesized by a simple one-step solution plasma process at room temperature using a mixture of benzene (C6H6) and organics containing halogen atoms as the precursors (i.e., hexafluorobenzene (C6F6), hexachlorobenzene (C6Cl6), and hexabromobenzene (C6Br6)). The experimental results demonstrated that ha...
Effect of microstructure on corrosion resistance and heat resistance of flame-resistant Ca-added magnesium alloy AZ61 (AZX612) were investigated. An extruded and twin-rolled casting magnesium alloys AZX612 were used with a view to better understanding the relationship between microstructure and these properties. The microstructures of the magnesium...
Films of the Mg(OH)2/Mg–Al layered double hydroxide composite were formed on the combustion-resistant magnesium alloy AMCa602 by steam coating and characterized by X-ray diffraction, Fourier-transform infrared spectroscopy, and scanning electron microscopy. The corrosion-resistance performances of the films in a 5 wt% NaCl solution were investigate...
Aligned, unidirectional, elongated pores were incorporated in Ti-6Al-4V products fabricated by electron beam melting in order to control the mechanical properties of the products such that they became suitable for biomedical applications. Unidirectional pores were successfully produced when the scan spacing of the electron beam was greater than the...
Bone microstructure is dominantly composed of anisotropic extracellular matrix (ECM) in which collagen fibers and epitaxially-oriented biological apatite (BAp) crystals are preferentially aligned depending on the bone anatomical position, resulting in exerting appropriate mechanical function. The regenerative bone in bony defects is however produce...
The development of the implant material which works much like bone must be an intrinsic approach to reduce the mechanical mismatch. Bone expresses the anisotropy of the mechanical characteristics based on the microstructual adaptation attributed to the apatite c-axis orientation corresponding to in vivo stress distribution. Therefore, the control o...
Estimates of the radii and solute concentrations of simulated microstructures containing ultrafine spherical precipitates were determined from isoconcentration surfaces and proximity histograms. The accuracy of the estimates of the solute concentrations and the radii of precipitates was found to depend on the size of precipitates. Optimized paramet...
The effect of high densities of dislocations on the formation behavior of two types of nano-scale clusters (nanoclusters), which are formed at room temperature or during pre-aging at ∼373 K in an Al–Mg–Si alloy, was investigated by atom probe tomography. Cold rolling was applied to modify the formation behavior and/or the characteristics of the nan...
It is known that the distribution of the charge-states as well as the evaporation field shift to higher values as the specimen temperature is decreased at a constant rate of evaporation. This study has explored the effect of Mg or Ag addition on the evaporation field of Al in terms of the charge state distribution of the field evaporated Al ions. T...
Co-Cr-Mo based alloys have been widely employed as heat resistant materials and as biomaterials for implants because of their high strength and superior wear resistance. In general, the alloys exhibit a very complicated composition-dependent microstructure containing stacking faults and related mechanical properties. Thus, the essential properties...
A series of simulated microstructures containing nanometer-scale precipitates was created with an atom probe simulator. These data were then analyzed with the proximity histogram and the maximum separation method to determine the influence of the particular analysis method. For simulated 2-nm-radius spherical precipitates, the optimized voxel size...
The quantification of the interaction between nanoclusters and dislocation motion has received relatively little experimental or theoretical research. In this work, the relationship between nanoclusters and dislocations was investigated by conducting tensile tests at different temperatures for a variety of nanoclusters in Al–Mg–Si alloys. Further,...
The characterization of nanoscale clusters (nanoclusters) was performed using differential scanning calorimetry (DSC) and
a three-dimensional atom probe (3DAP), to clarify the complicated aging behavior of an Al-Mg-Si alloy. The DSC results conducted
over the temperature range 223 to 473K revealed that two types of nanoclusters, i.e., Cluster(1) an...
The formation of nano-scale clusters (nanoclusters) prior to the precipitation of the
strengthening β" phase significantly influences the two-step aging behavior of Al-Mg-Si alloys. In
this work, two types of nanoclusters are found to be formed at different temperatures. The
characterization of these two nanoclusters has been performed from the vie...
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